C₉H₁₁NS₂*H₃N

Base Information

• Chemical Name: C₉H₁₁NS₂*H₃N
• CAS No.: 108654-39-3
• Molecular Formula: C₉H₁₁NS₂*H₃N
• Molecular Weight: 214.356
• Mol file: 108654-39-3.mol

Synonyms:

Chemical Property of C₉H₁₁NS₂*H₃N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₁₁NS₂*H₃N

There total 1 articles about C₉H₁₁NS₂*H₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2,5-Dimethylaniline (95-78-3) → C9H11NS2*H3N (108654-39-3)

Guidance literature:

With ammonia; In ethanol; at 20 ℃; for 1h;

DOI:10.3390/molecules16064527

Reference yield:

C9H11NS2*H3N (108654-39-3) → 4-(2',5'-Dimethylphenyl)-thiosemicarbazid (64374-53-4)

Guidance literature:

C₉H₁₁NS₂*H₃N; With sodium monochloroacetic acid; In ethanol; at 20 ℃; for 0.5h;

With hydrazine hydrate; In ethanol; at 20 ℃; for 1h;

DOI:10.3390/molecules16064527

Reference yield:

C9H11NS2*H3N (108654-39-3) → 4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde N4-(2,5-dimethylphenyl)thiosemicarbazone (1309469-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium monochloroacetic acid / ethanol / 0.5 h / 20 °C

1.2: 1 h / 20 °C

2.1: acetic acid / ethanol / 2 h / 20 °C

With sodium monochloroacetic acid; acetic acid; In ethanol;

DOI:10.3390/molecules16064527

upstream raw materials:

carbon disulfide

2,5-Dimethylaniline

Downstream raw materials:

4-[(10S)-dihydroartemisinin-10-oxy]benzaldehyde N₄-(2,5-dimethylphenyl)thiosemicarbazone

4-(2',5'-Dimethylphenyl)-thiosemicarbazid