C₆₃H₈₂N₄O₁₄Si

Base Information

Chemical Name:C₆₃H₈₂N₄O₁₄Si
CAS No.:1297295-87-4
Molecular Formula:C₆₃H₈₂N₄O₁₄Si
Molecular Weight:1147.45
Hs Code.:

C<sub>63</sub>H<sub>82</sub>N<sub>4</sub>O<sub>14</sub>Si

Synonyms:

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Chemical Property of C₆₃H₈₂N₄O₁₄Si

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Technology Process of C₆₃H₈₂N₄O₁₄Si

There total 8 articles about C₆₃H₈₂N₄O₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-41-3
t-Boc-L-valine

: C₅₃H₆₅N₃O₁₁Si

: 1297295-87-4
C₆₃H₈₂N₄O₁₄Si

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2010.11.165

Reference yield:

: 1297295-76-1
C₂₀H₂₁N₃O₇S

: 1297295-87-4
C₆₃H₈₂N₄O₁₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / toluene / 3 h / 0 - 20 °C

2: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 4 h / 0 °C

3: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; sodium hydrogencarbonate; benzotriazol-1-ol; caesium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2010.11.165

Reference yield:

: 898908-16-2
C₅H₁₃NO₂

: 1297295-87-4
C₆₃H₈₂N₄O₁₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: sodium carbonate / tetrahydrofuran; water / 16 h / 20 °C

2: sodium chlorite; sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl; H₂O₄P^(1-)*Na⁽³⁺⁾ / acetonitrile / 18 h / 40 °C

3: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

4: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C

5: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / toluene / 3 h / 0 - 20 °C

6: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 4 h / 0 °C

7: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; di-isopropyl azodicarboxylate; H₂O₄P^(1-)*Na⁽³⁺⁾; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; sodium hydrogencarbonate; sodium carbonate; benzotriazol-1-ol; caesium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2010.11.165