[(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone

Base Information

• Chemical Name: [(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone
• CAS No.: 1182735-06-3
• Molecular Formula: C₂₈H₂₆N₄O₄S
• Molecular Weight: 514.605

Synonyms:

Chemical Property of [(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone

Chemical Property:

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Useful:

Technology Process of [(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone

There total 1 articles about [(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(E)-4,4'-dicyanostilbene (5216-37-5) + C13H18N2O4S → [(4S,5S)-4,5-bis(4-cyanophenyl)-4,5-dihydroisoxazol-3-yl][(3aS,6R,7aR)-tetrahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazol-1,(4H)-yl]methanone (1182735-06-3) + C28H26N4O4S + (3aS,3'aS,6R,6'R,7aR,7'aR)-1,1'-[(2-oxidofurazan-2,4-diyl)bis(carbonyl)]bis[hexahydro-8,8-dimethyl-2,2-dioxido-3H-3a,6-methano-2,1-benzisothiazole]

Guidance literature:

With potassium hydrogencarbonate; In chloroform; at 20 ℃; optical yield given as %de; diastereoselective reaction;

DOI:10.1002/hlca.200800412

upstream raw materials:

(E)-4,4'-dicyanostilbene

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