C₃₄H₄₀N₂O₄

Base Information

Chemical Name:C₃₄H₄₀N₂O₄
CAS No.:1447825-73-1
Molecular Formula:C₃₄H₄₀N₂O₄
Molecular Weight:540.703
Hs Code.:

C<sub>34</sub>H<sub>40</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₄H₄₀N₂O₄

Chemical Property:

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Technology Process of C₃₄H₄₀N₂O₄

There total 9 articles about C₃₄H₄₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447825-68-4
C₃₃H₃₉NO₄Si

: 1447825-73-1
C₃₄H₄₀N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

1.2: 1 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

3.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

4.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

5.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

8.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

9.1: 29 h / Reflux

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; diisobutylaluminium hydride; sodium carbonate; Dess-Martin periodane; copper(II) sulfate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 3.1: |Grignard Reaction / 6.1: |Dess-Martin Oxidation / 9.1: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-71-9
C₃₅H₄₉NO₂SSi

: 1447825-73-1
C₃₄H₄₀N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

6: 29 h / Reflux

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 3: |Dess-Martin Oxidation / 6: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-91-3
C₂₇H₃₉NO₂SSi

: 1447825-73-1
C₃₄H₄₀N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

2: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

3: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

5: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

6: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

7: 29 h / Reflux

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 1: |Grignard Reaction / 4: |Dess-Martin Oxidation / 7: |Curtius Rearrangement;
DOI:10.1021/jm400542h