(3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

Base Information

Chemical Name:(3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate
CAS No.:122874-09-3
Molecular Formula:C₃₁H₄₅Cl₂N₂O₁₅P
Molecular Weight:787.582
Hs Code.:

(3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

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Chemical Property of (3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

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Technology Process of (3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

There total 2 articles about (3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113832-89-6,113833-09-3
Methyl 4-<2-<(1RS)-2-Benzyloxy-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propoxy>ethyl>benzoate

: 122874-09-3,122922-07-0,122922-08-1,122922-09-2
(3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / H₂ / 10percent Pd/C, 5percent Pd/CaCO₃ / ethyl acetate / 8 h / 760 Torr / Ambient temperature

2: triethylamine / CH₂Cl₂; toluene / 96 h / Ambient temperature

3: ammonia / CH₂Cl₂; toluene / Ambient temperature

With ammonia; hydrogen; triethylamine; Lindlar's catalyst; In dichloromethane; ethyl acetate; toluene;

Reference yield:

: 122874-05-9,122874-19-5
methyl 4-<2<(1RS)-3-hydroxy-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propoxy>ethyl>benzoate

: 122874-09-3,122922-07-0,122922-08-1,122922-09-2
(3RS,P-RS)-3-<2-(4-methoxycarbonylphenyl)ethoxy>-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)propyl N,N-bis(2-chloroethyl)phosphordiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂; toluene / 96 h / Ambient temperature

2: ammonia / CH₂Cl₂; toluene / Ambient temperature

With ammonia; triethylamine; In dichloromethane; toluene;