Technology Process of C27H42N2O9S3
There total 12 articles about C27H42N2O9S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
ethanol; water;
at 4 ℃;
DOI:10.1021/jm500602h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 2 h / 0 - 20 °C
2: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.33 h / 20 °C
3: sodium periodate / water; ethanol / 4 °C
With
sodium periodate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500602h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / ethyl acetate / 0.25 h / 20 °C
1.2: 12 h / Reflux
2.1: dichloromethane / 2 h / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.33 h / 20 °C
4.1: sodium periodate / water; ethanol / 4 °C
With
sodium periodate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm500602h
