4,3':5',4''-Terpyridine

Base Information

Chemical Name:4,3':5',4''-Terpyridine
CAS No.:106047-37-4
Molecular Formula:C15H11N3
Molecular Weight:233.26800
Hs Code.:

Synonyms:5',4'']Terpyridine;[4,3';

Suppliers and Price of 4,3':5',4''-Terpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
3,5-Di(pyridin-4-yl)pyridine
1g
$ 3126.60

Alichem
3,5-Di(pyridin-4-yl)pyridine
500mg
$ 1769.25

Alichem
3,5-Di(pyridin-4-yl)pyridine
250mg
$ 940.80

Total 15 raw suppliers

Chemical Property of 4,3':5',4''-Terpyridine

Chemical Property:

Melting Point:178 - 179 °C
PSA：38.67000
LogP:3.20560

Purity/Quality:

99% ^*data from raw suppliers

3,5-Di(pyridin-4-yl)pyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,3':5',4''-Terpyridine

There total 2 articles about 4,3':5',4''-Terpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 625-92-3
3,5-dibromopyridine

: 181219-01-2
4-pyridineboronic acid pinacol ester

: 106047-37-4
4,3′:5′,4″-terpyridine

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 96h; Heating;
DOI:10.1246/bcsj.75.559

Reference yield: 52.0%

: 625-92-3
3,5-dibromopyridine

: 93830-58-1
diethyl (pyridin-4-yl)borane

: 106047-37-4
4,3′:5′,4″-terpyridine

Guidance literature:: With potassium hydroxide; tetrabutylammomium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Heating;
DOI:10.1248/cpb.33.4755

Reference yield: 99.0%

: 106-46-7,84348-21-0
para-dichlorobenzene

: bis(ethylenediamine)palladium nitrate

: 106047-37-4
4,3′:5′,4″-terpyridine

: [(C₂H₈N₂Pd)6(C₁₅H₁₁N₃)4]⁽¹²⁺⁾*12NO₃^(1-)*C₆H₄Cl₂=[(C₂H₈N₂Pd)6(C₁₅H₁₁N₃)4](NO₃)12*C₆H₄Cl₂

Guidance literature:: In water-d2; C5H3N(C5H4N)2 suspended in D2O soln. of Pd complex; the mixt. heated at 80°C for 15 min; C6H4Cl2 added to the soln., stirred at room. temp. for 9 h; the excess of C6H4Cl2 filtered; not isolated; monitored by NMR;
DOI:10.1246/bcsj.75.559