2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine

Base Information

Chemical Name:2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine
CAS No.:139954-22-6
Molecular Formula:C₆₈H₉₂Ge₂N₆O₆P₂Si₄
Molecular Weight:1408.98
Hs Code.:

2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine

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Chemical Property of 2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine

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Technology Process of 2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine

There total 1 articles about 2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 97217-32-8
bis{(2,6-dimethylphenyl)(trimethylsilylamino)}germane(II)

: 26386-88-9
diphenyl phosphoryl azide

: 139954-22-6
2,2,6,6-tetrakis{(2,6-dimethylphenyl)(trimethylsilyl)amino}-4,4,8,8-tetraphenoxy-1,5-dioxa-3,7-λ(3.7)-diaza-4,8-diphospha-2,6-digermocine

Guidance literature:: In tetrahydrofuran; byproducts: N2; dropwise addn. of phosphorylazide soln. to germane soln. under N2 with stirring; stirring, 2 h; evapn.; pptn. filtration; washing (cold hexane); drying (vac.); elem. anal. (freshly prepd. product contains 1 mol THF per formula unit);;