(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane
CAS No.:850913-06-3
Molecular Formula:C₅₇H₆₇N₁₁O₃
Molecular Weight:954.231
Hs Code.:

(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

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Chemical Property of (S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

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Technology Process of (S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

There total 8 articles about (S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 850913-07-4
1-(3-methyl-10,11,2,13-tetrahydropyrido[3,2-α:2',3'-c]phenzine)-1,4,7,10-tetraazacyclododecane

: 36293-01-3
2-chloro-N-((1S)-1-phenylethyl)acetamide

: 850913-06-3
(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: With potassium carbonate; potassium iodide; In dichloromethane; acetonitrile; Heating;
DOI:10.1039/b418964g

Reference yield:

: 850912-90-2
2-methyl-1,10-phenanthroline-5,6-dione

: 850913-06-3
(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / ethanol / 5 h / Heating

2: SeO₂ / dioxane / 4 h / Heating

3: 65 percent / NaBH₄ / CHCl₃; ethanol / 2 h / Heating

4: 76 percent / KI; K₂CO₃ / acetonitrile; CH₂Cl₂ / Heating

5: 82 percent / CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

6: 48 percent / K₂CO₃; KI / acetonitrile; CH₂Cl₂ / Heating

With sodium tetrahydroborate; selenium(IV) oxide; potassium carbonate; trifluoroacetic acid; potassium iodide; In 1,4-dioxane; ethanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1039/b418964g

Reference yield:

: 850912-92-4
7-methyl-10,11,12,13-tetrahydrodipyrido[3,2a:2',3'-c]phenazine

: 850913-06-3
(S,S,S)-1-(3-methyl-10,11,12,13-tetrahydrodipyrido[3,2-a:2',3'-c]phenazine)-4,7,10-tris[N-(1-phenylethyl)carbamoylmethyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 5 steps

1: SeO₂ / dioxane / 4 h / Heating

2: 65 percent / NaBH₄ / CHCl₃; ethanol / 2 h / Heating

3: 76 percent / KI; K₂CO₃ / acetonitrile; CH₂Cl₂ / Heating

4: 82 percent / CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

5: 48 percent / K₂CO₃; KI / acetonitrile; CH₂Cl₂ / Heating

With sodium tetrahydroborate; selenium(IV) oxide; potassium carbonate; trifluoroacetic acid; potassium iodide; In 1,4-dioxane; ethanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1039/b418964g