C₄₃H₇₂O₇Si₃

Base Information

Chemical Name:C₄₃H₇₂O₇Si₃
CAS No.:1310025-42-3
Molecular Formula:C₄₃H₇₂O₇Si₃
Molecular Weight:785.297
Hs Code.:

C<sub>43</sub>H<sub>72</sub>O<sub>7</sub>Si<sub>3</sub>

Synonyms:

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Chemical Property of C₄₃H₇₂O₇Si₃

Chemical Property:

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Technology Process of C₄₃H₇₂O₇Si₃

There total 9 articles about C₄₃H₇₂O₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310025-41-2
C₄₃H₇₄O₆Si₃

: 1310025-42-3
C₄₃H₇₂O₇Si₃

Guidance literature:: C₄₃H₇₄O₆Si₃; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 20 ℃; for 1.33333h; Inert atmosphere;

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; acetonitrile; for 0.75h; Inert atmosphere; Cooling with ice;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-34-3
C₃₄H₄₄O₅Si

: 1310025-42-3
C₄₃H₇₂O₇Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.03 h / Inert atmosphere; Cooling with ice

1.2: 0.33 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; pentane / 0.23 h / -78 - 0 °C / Inert atmosphere

2.2: 0.77 h / -78 °C / Inert atmosphere

2.3: -78 °C

3.1: pyridinium p-toluenesulfonate / 3 h / 45 °C / Inert atmosphere

4.1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: magnesium / diethyl ether / Inert atmosphere; Reflux

6.2: 1.22 h / -78 °C / Inert atmosphere

6.3: 70 h / 20 °C / Inert atmosphere

7.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.68 h / Inert atmosphere; Cooling with ice

8.1: lithium dihydronaphthylide radical / tetrahydrofuran / 1 h / -30 - -10 °C / Inert atmosphere

9.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 1.33 h / 20 °C / Inert atmosphere

9.2: 0.75 h / Inert atmosphere; Cooling with ice

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; lithium dihydronaphthylide radical; magnesium; diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; pentane;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-61-6
C₄₈H₆₄O₈Si

: 1310025-42-3
C₄₃H₇₂O₇Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: magnesium / diethyl ether / Inert atmosphere; Reflux

2.2: 1.22 h / -78 °C / Inert atmosphere

2.3: 70 h / 20 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.68 h / Inert atmosphere; Cooling with ice

4.1: lithium dihydronaphthylide radical / tetrahydrofuran / 1 h / -30 - -10 °C / Inert atmosphere

5.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 1.33 h / 20 °C / Inert atmosphere

5.2: 0.75 h / Inert atmosphere; Cooling with ice

With 1H-imidazole; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; lithium dihydronaphthylide radical; magnesium; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1021/ja203034k