iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

Base Information

Chemical Name:iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane
CAS No.:125849-71-0
Molecular Formula:C₅₄H₈₇ISn
Molecular Weight:981.899
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

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Technology Process of iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

There total 1 articles about iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: tin(IV) iodide

: 35383-91-6
2,4,6-tri-tert-butylphenyllithium

: 125849-71-0
iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

Guidance literature:: In petroleum ether; byproducts: LiI; addn. of SnI4 in petroleum ether to suspn. of org. compd. in petroleum ether (-78°C), stirring (0.5 h, -78°C), stirring (room temp., 12 h); removal of LiI, cooling (-25°C), recrystn. (petroleum ether); elem. anal.;

Reference yield: 11.0%

: 125849-71-0
iodo(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

: 917-54-4
methyllithium

: 125849-72-1
methyl(2,4,6-tri-tert-butylphenyl)bis{2-methyl-2(3,5-di-tert-butylphenyl)propyl}stannane

Guidance literature:: In diethyl ether; toluene; byproducts: LiI; addn. of soln. of MeLi in ether to Sn-compd. in toluene (0°C), stirring (0°C, 1 h and room temp., 1 h); solvent exchange (petroleum ether), filtn. LiI, recrystn. (petroleum ether); elem. anal.;