C₄₅H₆₆N₄O₉Si

Base Information

Chemical Name:C₄₅H₆₆N₄O₉Si
CAS No.:1381817-13-5
Molecular Formula:C₄₅H₆₆N₄O₉Si
Molecular Weight:835.126
Hs Code.:

C<sub>45</sub>H<sub>66</sub>N<sub>4</sub>O<sub>9</sub>Si

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Chemical Property of C₄₅H₆₆N₄O₉Si

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Technology Process of C₄₅H₆₆N₄O₉Si

There total 16 articles about C₄₅H₆₆N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90819-30-0
(S)-2-((tert-butoxycarbonyl)amino)-3-(3-hydroxyphenyl)propanoic acid

: 1381817-13-5
C₄₅H₆₆N₄O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 18 h / 20 °C

2.1: 1H-imidazole / acetone / 24 h / 20 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.42 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 18 h

5.1: sodium hydride / tetrahydrofuran / 18 h / 50 °C / Inert atmosphere

6.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.2: 0 °C / Inert atmosphere

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 18 h / 20 °C

8.1: Grubbs catalyst first generation / dichloromethane / 24 h / Reflux; Inert atmosphere

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; sodium hydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;

Reference yield:

: (S)-hexahydro-pyridazine-3-carboxylic acid 2,2,2-trichloro-ethyl ester

: 1381817-13-5
C₄₅H₆₆N₄O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 18 h / 20 °C

2.1: 1H-imidazole / acetone / 24 h / 20 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.42 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 18 h

5.1: sodium hydride / tetrahydrofuran / 18 h / 50 °C / Inert atmosphere

6.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.2: 0 °C / Inert atmosphere

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 18 h / 20 °C

8.1: Grubbs catalyst first generation / dichloromethane / 24 h / Reflux; Inert atmosphere

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; sodium hydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;

Reference yield:

: 1381814-97-6
(S)-1-{(S)-2-[(S)-2-tert-butoxycarbonylamino-3-(4-methoxy-phenyl)-propionylamino]-3-[3-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionyl}-hexahydro-pyridazine-3-carboxylic acid but-3-enyl ester

: 1381817-13-5
C₄₅H₆₆N₄O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 18 h / 20 °C

3.1: Grubbs catalyst first generation / dichloromethane / 24 h / Reflux; Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Grubbs catalyst first generation; In dichloromethane; acetonitrile;