C₃₉H₅₂O₅Si

Base Information

Chemical Name:C₃₉H₅₂O₅Si
CAS No.:1314123-83-5
Molecular Formula:C₃₉H₅₂O₅Si
Molecular Weight:628.924
Hs Code.:

C<sub>39</sub>H<sub>52</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₃₉H₅₂O₅Si

Chemical Property:

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Technology Process of C₃₉H₅₂O₅Si

There total 16 articles about C₃₉H₅₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314123-86-8
6-((2S,3R,5S)-2-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-3,5-dimethylheptyl)-2,2-dimethyl-4H-1,3-dioxin-4-one

: 1314123-83-5
C₃₉H₅₂O₅Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: methanol; ammonium fluoride / 24 h / 40 °C / Inert atmosphere

2.1: ortho-nitrophenyl selenocyanate; tributylphosphine / tetrahydrofuran / 0.5 h / 23 °C / Inert atmosphere

2.2: 12 h / 0 °C / Inert atmosphere

3.1: dichloromethane / 4.5 h / 0 - 20 °C / Inert atmosphere

4.1: pyridine hydrofluoride / tetrahydrofuran / 48 h / 0 - 20 °C / Inert atmosphere

5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.75 h / -78 - -40 °C / Inert atmosphere

6.1: hydrogen fluoride; water / acetonitrile / 18 h / 20 °C / Inert atmosphere

7.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

7.2: Inert atmosphere

8.1: potassium carbonate / acetonitrile / 2 h / 70 °C / Inert atmosphere

9.1: 1H-imidazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

10.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 22 h / Inert atmosphere

11.1: tributylphosphine / tetrahydrofuran / 1 h / Inert atmosphere

12.1: dihydrogen peroxide / tetrahydrofuran; water / 18 h / 0 °C / Inert atmosphere

13.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Reflux

14.1: platinum(IV) oxide; hydrogen / ethyl acetate / 1.5 h

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; platinum(IV) oxide; ammonium fluoride; ortho-nitrophenyl selenocyanate; tributylphosphine; pyridine hydrofluoride; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; potassium tert-butylate; water; hydrogen; dihydrogen peroxide; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile; 2.1: Grieco elimination / 2.2: Grieco elimination;
DOI:10.1002/anie.201102037

Reference yield:

: 1314123-77-7
(5S,6R,8S)-ethyl 5-hydroxy-6,8-dimethyl-3-oxodec-9-enoate

: 1314123-83-5
C₃₉H₅₂O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.75 h / -78 - -40 °C / Inert atmosphere

2.1: hydrogen fluoride; water / acetonitrile / 18 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

3.2: Inert atmosphere

4.1: potassium carbonate / acetonitrile / 2 h / 70 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 22 h / Inert atmosphere

7.1: tributylphosphine / tetrahydrofuran / 1 h / Inert atmosphere

8.1: dihydrogen peroxide / tetrahydrofuran; water / 18 h / 0 °C / Inert atmosphere

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Reflux

10.1: platinum(IV) oxide; hydrogen / ethyl acetate / 1.5 h

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; platinum(IV) oxide; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; potassium tert-butylate; water; hydrogen; dihydrogen peroxide; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201102037

Reference yield:

: 1314123-80-2
(2R,6S)-ethyl 2-((1S,2S,5S)-2-(3-(benzyloxy)propyl)-1-(tert-butyldimethylsilyloxy)-4-((tert-butyldiphenylsilyloxy)methyl)-5-methylcyclohex-3-enyl)-6-((2R,4S)-4-methylhex-5-en-2-yl)-4-oxotetrahydro-2H-pyran-3-carboxylate

: 1314123-83-5
C₃₉H₅₂O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen fluoride; water / acetonitrile / 18 h / 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / Inert atmosphere

2.2: Inert atmosphere

3.1: potassium carbonate / acetonitrile / 2 h / 70 °C / Inert atmosphere

4.1: 1H-imidazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

5.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 22 h / Inert atmosphere

6.1: tributylphosphine / tetrahydrofuran / 1 h / Inert atmosphere

7.1: dihydrogen peroxide / tetrahydrofuran; water / 18 h / 0 °C / Inert atmosphere

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Reflux

9.1: platinum(IV) oxide; hydrogen / ethyl acetate / 1.5 h

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; platinum(IV) oxide; tributylphosphine; hydrogen fluoride; potassium tert-butylate; water; hydrogen; dihydrogen peroxide; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201102037