NiI₂((CH₃)2BrC₆H₂NC)2

Base Information

Chemical Name:NiI₂((CH₃)2BrC₆H₂NC)2
CAS No.:148683-39-0
Molecular Formula:C₁₈H₁₆Br₂I₂N₂Ni
Molecular Weight:732.645
Hs Code.:

NiI<sub>2</sub>((CH<sub>3</sub>)2BrC<sub>6</sub>H<sub>2</sub>NC)2

Synonyms:

Suppliers and Price of NiI₂((CH₃)2BrC₆H₂NC)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of NiI₂((CH₃)2BrC₆H₂NC)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of NiI₂((CH₃)2BrC₆H₂NC)2

There total 1 articles about NiI₂((CH₃)2BrC₆H₂NC)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13462-90-3
nickel(II) iodide

: 24139-49-9
5-bromo-2-isocyano-1,3-dimethylbenzene

: 148683-39-0,139010-67-6
NiI₂((CH₃)2BrC₆H₂NC)2

Guidance literature:: In dichloromethane; a mixt. of NiI2 and isocyanide-compd. in CH2Cl2 is stirred at room temp.; after 1 h the mixt. is filtered, solvent is removed in vac., the residue is crystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1246/bcsj.64.3376

Reference yield: 87.0%

: 148683-39-0,139010-67-6
NiI₂((CH₃)2BrC₆H₂NC)2

: 24139-49-9
5-bromo-2-isocyano-1,3-dimethylbenzene

: mercury

: {Ni((CH₃)2C₆H₂(Br)NC)4HgI₂}2

Guidance literature:: In acetonitrile; a mixt. of trans-NiI2(4-Br-2,6-Me2C6H2NC)2, 4-bromo-2,6-dimethylphenylisocyanide and Hg is stirred for 2.5 h at room temp.; the organic layer is dried, residue is extd. with benzene, the solvent is concd., hexane added, giving crystals, recrystd. from benzene-hexane; elem. anal.;
DOI:10.1246/bcsj.64.3376

Reference yield: 77.0%

: 148683-39-0,139010-67-6
NiI₂((CH₃)2BrC₆H₂NC)2

: 24139-49-9
5-bromo-2-isocyano-1,3-dimethylbenzene

: 38548-52-6
Ni(Br(CH₃)2C₆H₂NC)4

Guidance literature:: With sodium amalgam; In tetrahydrofuran; stirring soln. of Ni-complex and org. compd. with sodium amalgame in THF (2 h, room temp.); decanting, solvent removal, chromy. (alumina, benzene), solvent removal, crystn. (benzene-hexane); elem. anal.;
DOI:10.1246/bcsj.66.778