1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct

Base Information

• Chemical Name: 1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct
• CAS No.: 511270-36-3
• Molecular Formula: C₇H₈*C₃₀H₂₅O₂Sb
• Molecular Weight: 631.418
• Mol file: 511270-36-3.mol

Synonyms:

Chemical Property of 1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct

Chemical Property:

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Technology Process of 1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct

There total 1 articles about 1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

pentaphenylantimony (2170-05-0) + toluene (108-88-3,15644-74-3,16713-13-6) + recorcinol (108-46-3) → 1-(tetraphenylstiboxy)-3-oxybenzene toluene adduct (511270-36-3)

Guidance literature:

In toluene; byproducts: C6H6; Ph5Sb + resorcin (1:1 molar ratio) heated in toluene (100°C, 1 h); cooled to room temp.; petroleum ether added; cooled to -18°C; crystals filtered off; dried;

DOI:10.1023/A:1021198513120

upstream raw materials:

pentaphenylantimony

toluene

recorcinol