(P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉

Base Information

Chemical Name:(P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉
CAS No.:98991-67-4
Molecular Formula:C₄₈H₅₃BrOP₂Pd
Molecular Weight:896.204
Hs Code.:

(P(C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)3)2BrPdC<sup>(2)</sup>H<sub>2</sub>COC<sub>4</sub>H<sub>9</sub>

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Chemical Property of (P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉

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Technology Process of (P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉

There total 1 articles about (P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99016-52-1
1-bromo-1-deuterio-3,3-dimethyl-2-butanone

: 29032-56-2
tetrakis(tris(4-methyl)phenyl)phosphinepalladium

: 98991-67-4
(P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉

Guidance literature:: In benzene; to a soln. of complex in benzene under Ar at 25°C was added ketone, 1.0 h; concd. in vac., solid was washed with hexane, recrystd. from THF/hexane;
DOI:10.1021/om00132a022

Reference yield:

: 98991-62-9
(P(C₆H₅)3)2BrPdCH₂COC₄H₉*CH₂Cl₂

: 98991-67-4
(P(C₆H₄CH₃)3)2BrPdC⁽²⁾H₂COC₄H₉

: (C₆H₄CH₃)3PC⁽²⁾HCOC₄H₉

: 29032-56-2
tetrakis(tris(4-methyl)phenyl)phosphinepalladium

: 288390-74-9
3,3-dimethyl-1-(triphenylphosphanylidene)butan-2-one

Guidance literature:: With t-BuOK-d9; In tetrahydrofuran-d8; to an argon-flushed NMR tube at -95°C are added Pd compds. and THF-d8 and t-BuOK-d9, seales under vac. and warmed to -78.defree.C; monitored by (1)H NMR at -63°C; Kinetics;
DOI:10.1021/om00132a022