(π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride

Base Information

Chemical Name:(π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride
CAS No.:921624-92-2
Molecular Formula:C₂₆H₂₇Cl₂F₆NO₂PRh
Molecular Weight:704.282
Hs Code.:

(π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride

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Chemical Property of (π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride

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Technology Process of (π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride

There total 1 articles about (π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 921624-75-1
3-methyl-2-{2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy}-2,3-dihydro-1,3,2-benzoxazaphosphole

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 921624-92-2
(π-pentamethylcyclopentadienyl)(3-methyl-2-(2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy)-2,3-dihydro-1,3,2-benzoxazaphosphole)rhodium dichloride

Guidance literature:: In dichloromethane; (Ar); using Schlenk techniques; addn. of 3-methyl-2-(2,2,2-trifluoro-1-(3-(trifluoromethyl)phenyl)ethoxy)-2,3-dihydro-1,3,2-benzoxazaphopshole to soln. of (Rh(C5Me5)Cl2)2 in CH2Cl2; stirring for 1 h at room temp.; concn. in vac., addn. of pentane, crystn., filtration, drying in vac., elem. anal.;
DOI:10.1016/j.jorganchem.2006.08.098