hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

Base Information

Chemical Name:hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)
CAS No.:125566-19-0
Molecular Formula:C₄₃H₅₆MoP₂S₃
Molecular Weight:827.003
Hs Code.:

Synonyms:

Suppliers and Price of hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

There total 1 articles about hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1541-10-2
mesitylthiol

: MoBr₂(NNH₂)(PMe₂Ph)3

: 125566-19-0
hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

Guidance literature:: With (C₂H₅)3N; In methanol; byproducts: NH(C2H5)3Br, P(CH3)2C6H5, N2; 3 equiv. of each, HSC6H2(CH3)3 and (C2H5)3N, were added to a methanolic suspension of the bromo-complex, heated at 60°C and allowed to cool to room temp. within 3 h; further by-product: H2;; the ppt. was washed twice with MeOH and dried in vac.; elem. anal.;;
DOI:10.1039/DT9910001813

Reference yield: 56.0%

: 125566-19-0
hydridobis(dimethylphenylphosphine)tris(2,4,6-trimethylthiophenolato)molybdenum(IV)

: 125566-21-4
dicarbonylbis(dimethylphenylphosphine)bis(2,4,6-trimethylthiophenolato)molybdenum(II)

Guidance literature:: With CO; In hexane; bubbling CO (3 h), stirring under CO (18 h); partial evapn. (vac.), crystn. on layering with MeOH (-20°C, 24 h), collection, washing (MeOH), drying (vac.); elem. anal.;
DOI:10.1039/DT9910002519