3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

Base Information

Chemical Name:3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile
CAS No.:35920-81-1
Molecular Formula:C₁₇H₂₁NO₅
Molecular Weight:319.357
Hs Code.:

Synonyms:

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Chemical Property of 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

Chemical Property:

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Technology Process of 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

There total 1 articles about 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35920-81-1
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

Guidance literature:: entspr. Anhydroverb., KCN;
DOI:10.1007/BF00912947

Reference yield: 65.7%

: 35920-81-1
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

: 887473-59-8
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-xylo-hept-5-ulofuranonitrile

Guidance literature:: With 3 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 3h;
DOI:10.1080/07328300500471770

Reference yield:

: 35920-81-1
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-gluco-heptfuranonitrile

: 3-(3-O-benzyl-β-D-xylo-tetrofuranos-4-yl)-1H-pyrazole-4-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 65.7 percent / pyridinium chlorochromate; molecular sieves 3 Angstroem / CH₂Cl₂ / 3 h

2: 72 percent / tetrahydrofuran / 2 h / 20 °C

3: 94 percent / hydrazine hydrate / ethanol / 0.25 h / 20 °C

4: trifluoroacetic acid; acetic acid / H₂O / 8 h / 20 °C

With 3 A molecular sieve; hydrazine hydrate; acetic acid; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1080/07328300500471770