C₄₄H₅₁N₃O₁₇

Base Information

Chemical Name:C₄₄H₅₁N₃O₁₇
CAS No.:155434-90-5
Molecular Formula:C₄₄H₅₁N₃O₁₇
Molecular Weight:893.899
Hs Code.:

C<sub>44</sub>H<sub>51</sub>N<sub>3</sub>O<sub>17</sub>

Synonyms:

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Chemical Property of C₄₄H₅₁N₃O₁₇

Chemical Property:

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Technology Process of C₄₄H₅₁N₃O₁₇

There total 14 articles about C₄₄H₅₁N₃O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50622-78-1
Benzyl 4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-methylpyrrole-2-carboxylate

: 155434-90-5
C₄₄H₅₁N₃O₁₇

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / H₂ / Pd-on-charcoal / methanol / 4 h / Ambient temperature

2: oxalyl chloride / CH₂Cl₂ / 0.5 h

3: N,N-dimethylaniline / CH₂Cl₂ / 1.) room temperature, 30 min, 2.) reflux, 10 min

4: SO₂Cl₂ / CH₂Cl₂ / 0.25 h

5: AcONa / 1 h / 75 °C

6: 1.) stannic chloride, 2.) p-TsOH*H₂O, AgOAc / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) THF, room temperature, 12 h

7: AcOH, Zn / 0.33 h

With sulfuryl dichloride; oxalyl dichloride; hydrogen; silver(I) acetate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; acetic acid; N,N-dimethyl-aniline; zinc; palladium on activated charcoal; In methanol; dichloromethane;

Reference yield:

: 75975-54-1
tert-butyl 3,3'-bis<(methoxycarbonyl)methyl>-4,4'-bis<β-(methoxycarbonyl)ethyl>-5-<(benzyloxy)carbonyl>dipyrrylmethane-5-carboxylate

: 155434-90-5
C₄₄H₅₁N₃O₁₇

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / stannic chloride / CH₂Cl₂ / 1.5 h / 0 °C

2: 100 percent / NaHCO₃, I₂, KI / CH₂Cl₂; H₂O / 0.33 h

3: 1.) stannic chloride, 2.) p-TsOH*H₂O, AgOAc / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) THF, room temperature, 12 h

4: AcOH, Zn / 0.33 h

With iodine; silver(I) acetate; tin(IV) chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; potassium iodide; zinc; In dichloromethane; water;

Reference yield:

: 107751-49-5
4-(2-Methoxycarbonyl-ethyl)-3-methoxycarbonylmethyl-5-methyl-1H-pyrrole-2-carboxylic acid

: 155434-90-5
C₄₄H₅₁N₃O₁₇

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl chloride / CH₂Cl₂ / 0.5 h

2: N,N-dimethylaniline / CH₂Cl₂ / 1.) room temperature, 30 min, 2.) reflux, 10 min

3: SO₂Cl₂ / CH₂Cl₂ / 0.25 h

4: AcONa / 1 h / 75 °C

5: 1.) stannic chloride, 2.) p-TsOH*H₂O, AgOAc / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) THF, room temperature, 12 h

6: AcOH, Zn / 0.33 h

With sulfuryl dichloride; oxalyl dichloride; silver(I) acetate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; acetic acid; N,N-dimethyl-aniline; zinc; In dichloromethane;