Benzenepropanol, b-[2-[2-(diethylamino)ethoxy]phenoxy]-a-methyl-

Base Information

Chemical Name:Benzenepropanol, b-[2-[2-(diethylamino)ethoxy]phenoxy]-a-methyl-
CAS No.:106063-83-6
Molecular Formula:C22H31NO3
Molecular Weight:357.493
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanol, b-[2-[2-(diethylamino)ethoxy]phenoxy]-a-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenepropanol, b-[2-[2-(diethylamino)ethoxy]phenoxy]-a-methyl-

There total 5 articles about Benzenepropanol, b-[2-[2-(diethylamino)ethoxy]phenoxy]-a-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106063-79-0
3-<2-<2-(diethylamino)ethoxy>phenoxy>-4-phenylbutan-2-one

: 106063-83-6
3-<2-<2-(diethylamino)ethoxy>phenoxy>-4-phenylbutan-2ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Heating;
DOI:10.1021/jm00388a005

Reference yield:

: 22965-96-4
(Z)-3-bromo-4-phenyl-3-buten-2-one

: 106063-83-6
3-<2-<2-(diethylamino)ethoxy>phenoxy>-4-phenylbutan-2ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) K₂CO₃, 2.) 10percent aq. NaOH / 1.) acetone, reflux, 4 h. 2.) ethyl ether

2: 67 percent / acetone / 35 h / Heating

3: 72 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

4: 62 percent / LiAlH₄ / diethyl ether / 3 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate; palladium on activated charcoal; In diethyl ether; ethanol; acetone;
DOI:10.1021/jm00388a005

Reference yield:

: 57150-77-3,68876-74-4
(Z)-3-<2-<2-(diethylamino)ethoxy>phenoxy>-4-phenyl-3-buten-2-one

: 106063-83-6
3-<2-<2-(diethylamino)ethoxy>phenoxy>-4-phenylbutan-2ol

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

2: 62 percent / LiAlH₄ / diethyl ether / 3 h / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jm00388a005