ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate

Base Information

• Chemical Name: ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate
• CAS No.: 1445718-97-7
• Molecular Formula: C₃₂H₄₁N₅O₆
• Molecular Weight: 595.692

Synonyms:

Chemical Property of ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate

Chemical Property:

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Useful:

Technology Process of ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate

There total 1 articles about ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate (1445712-43-5) → ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[3H2]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate (1445718-97-7)

Guidance literature:

With tritium; dimethylphenylphosphine(1,5-cyclooctadiene)[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene]iridium(I) hexafluorophosphate; In dichloromethane; for 2h; under 277.528 Torr; Autoclave;

DOI:10.1002/jlcr.3028

Reference yield:

ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[3H2]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate (1445718-97-7) → ethyl 2-((R)-1-cyclohexyl-2-((S)-2-(4-((Z)-N'-hydroxycarbamimidoyl)-3,5-[3H2]benzylcarbamoyl)azetidin-1-yl)-2-oxoethylamino)acetate (1445718-99-9)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In tetrahydrofuran; at 40 ℃;

DOI:10.1002/jlcr.3028

Reference yield:

ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)-3,5-[3H2]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate (1445718-97-7) → ethyl 2-((R)-2-((S)-2-(4-carbamimidoyl-3,5-[3H2]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate (1445712-50-4)

Guidance literature:

With hydrogen; palladium(II) hydroxide; In ethanol; water; for 1.5h;

DOI:10.1002/jlcr.3028

upstream raw materials:

ethyl 2-((R)-2-((S)-2-(4-((Z)-N'-(benzyloxycarbonyl)carbamimidoyl)benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate

Downstream raw materials:

ethyl 2-((R)-1-cyclohexyl-2-((S)-2-(4-((Z)-N'-hydroxycarbamimidoyl)-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-2-oxoethylamino)acetate

ethyl 2-((R)-2-((S)-2-(4-carbamimidoyl-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetate

2-((R)-2-((S)-2-(4-carbamimidoyl-3,5-[³H₂]benzylcarbamoyl)azetidin-1-yl)-1-cyclohexyl-2-oxoethylamino)acetic acid

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