N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

Base Information

Chemical Name:N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester
CAS No.:155711-42-5
Molecular Formula:C₁₀₆H₁₇₁N₂O₁₈P
Molecular Weight:1792.5
Hs Code.:

N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

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Chemical Property of N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

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Technology Process of N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

There total 2 articles about N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 87357-76-4
(R)-3-(dodecanoyloxy)tetradecanoic acid

: 155711-41-4
(S)-3-[(2R,3R,4R,5S,6R)-3-Amino-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-2-tetradecanoylamino-propionic acid benzyl ester

: 155711-42-5
N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1248/cpb.41.1879

Reference yield:

: 87357-76-4
(R)-3-(dodecanoyloxy)tetradecanoic acid

: (S)-3-[(3R,4R,5S,6R)-3-Amino-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-4-hydroxy-tetrahydro-pyran-2-yloxy]-2-tetradecanoylamino-propionic acid benzyl ester

: 155711-42-5
N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 15h; Yield given; Ambient temperature;
DOI:10.1248/cpb.44.2268

Reference yield:

: 155711-42-5
N-tetradecanoyl-O-<6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-2-<(R)-3-tetradecanoyloxytetradecanoylamino>-β-D-glucopyranosyl>-L-serine benzyl ester

: (R)-3-Tetradecanoyloxy-tetradecanoic acid (2R,3R,4R,5S,6R)-2-((S)-2-carboxy-2-tetradecanoylamino-ethoxy)-5-(diphenoxy-phosphoryloxy)-6-hydroxymethyl-3-((R)-3-tetradecanoyloxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

Guidance literature:: With platinum(IV) oxide; hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) MeOH, 40 deg C, 6 h, 2.) MeOH, 40 deg C, 24 h;
DOI:10.1248/cpb.41.1879