C₅₈H₅₃NO₃

Base Information

Chemical Name:C₅₈H₅₃NO₃
CAS No.:1246452-39-0
Molecular Formula:C₅₈H₅₃NO₃
Molecular Weight:812.064
Hs Code.:

C<sub>58</sub>H<sub>53</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₅₈H₅₃NO₃

Chemical Property:

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Technology Process of C₅₈H₅₃NO₃

There total 4 articles about C₅₈H₅₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49617-79-0
1,3-diiodo-5-methylbenzene

: 1246452-39-0
C₅₈H₅₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 70 °C

2.1: hydrazine hydrate / ethanol / Reflux

2.2: 20 °C

2.3: 20 °C

3.1: triethylamine / N,N-dimethyl-formamide / 20 °C

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 1.1: Williamson synthesis / 4.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242

Reference yield:

: 1246452-32-3
N-[3-(3,5-diiodophenoxy)propyl]phthalimide

: 1246452-39-0
C₅₈H₅₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / ethanol / Reflux

1.2: 20 °C

1.3: 20 °C

2.1: triethylamine / N,N-dimethyl-formamide / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 3.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242

Reference yield:

: 1246452-33-4
C₉H₁₁I₂NO

: 1246452-39-0
C₅₈H₅₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 20 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242