1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene

Base Information

Chemical Name:1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene
CAS No.:425394-72-5
Molecular Formula:C₈H₆Br₃Cl
Molecular Weight:377.301
Hs Code.:
DSSTox Substance ID:DTXSID101258538

Synonyms:1-bromo-2,3-bis(bromomethyl)-4-chlorobenzene;DTXSID101258538;425394-72-5

Suppliers and Price of 1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:375.76877
Heavy Atom Count:12
Complexity:142

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1Cl)CBr)CBr)Br

Technology Process of 1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene

There total 3 articles about 1-Bromo-2,3-bis(bromomethyl)-4-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22364-25-6
4-bromo-2,3-dimethylaniline

: 425394-72-5
1-chloro-4-bromo-2,3-bis(bromomethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; HCl; H₂SO₄ / H₂O; acetic acid / 0.25 h

1.2: 65 percent / HCl; CuCN / H₂O; acetic acid / 1 h / Heating

2.1: NBS

With hydrogenchloride; N-Bromosuccinimide; sulfuric acid; sodium nitrite; In water; acetic acid; 1.2: Sandmeyer reaction;
DOI:10.1021/jo010858m

Reference yield:

: 22369-96-6
4-bromo-2,3-dimethylacetanilide

: 425394-72-5
1-chloro-4-bromo-2,3-bis(bromomethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / HCl / ethanol / Heating

2.1: sodium nitrite; HCl; H₂SO₄ / H₂O; acetic acid / 0.25 h

2.2: 65 percent / HCl; CuCN / H₂O; acetic acid / 1 h / Heating

3.1: NBS

With hydrogenchloride; N-Bromosuccinimide; sulfuric acid; sodium nitrite; In ethanol; water; acetic acid; 2.2: Sandmeyer reaction;
DOI:10.1021/jo010858m