1,16-bis-1,4,7,10,13,16-hexaoxahexadecane

Base Information

Chemical Name:1,16-bis-1,4,7,10,13,16-hexaoxahexadecane
CAS No.:130740-01-1
Molecular Formula:C₂₈H₃₄O₁₀
Molecular Weight:530.572
Hs Code.:

1,16-bis<p-(2-carboxyvinyl)phenyl>-1,4,7,10,13,16-hexaoxahexadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,16-bis-1,4,7,10,13,16-hexaoxahexadecane

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Technology Process of 1,16-bis-1,4,7,10,13,16-hexaoxahexadecane

There total 2 articles about 1,16-bis-1,4,7,10,13,16-hexaoxahexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.2%

: 57602-02-5
1,14-dibromo-3,6,9,12-tetraoxatetradecane

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 130740-01-1
1,16-bis-1,4,7,10,13,16-hexaoxahexadecane

Guidance literature:: With sodium hydroxide; In ethanol; for 26h; Heating;
DOI:10.1246/bcsj.63.1623

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 130740-01-1
1,16-bis-1,4,7,10,13,16-hexaoxahexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 32.1 percent / piperidine / pyridine / 7 h / 100 °C

2: 10.2 percent / NaOH / aq. ethanol / 26 h / Heating

With piperidine; sodium hydroxide; In pyridine; ethanol;
DOI:10.1246/bcsj.63.1623