IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2

Base Information

Chemical Name:IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2
CAS No.:143202-26-0
Molecular Formula:C₅₁H₄₆ClIrN₂P₂
Molecular Weight:976.56
Hs Code.:

IrHCl(C<sub>6</sub>H<sub>5</sub>NC(C<sub>2</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2

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Suppliers and Price of IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2

Chemical Property:

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Technology Process of IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2

There total 2 articles about IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 24846-85-3,28060-70-0,77448-67-0,16971-01-0
IrHCl2(PPh3)3

: 6944-19-0
N,N'-diphenylpropionimidamide

: 143202-26-0
chloro(N,N'-diphenylpropioamidinato)hydridobis(triphenylphosphine)iridium(III)

Guidance literature:: With triethylamine; In benzene; under N2: heating of (IrHCl2(P(C6H5)3)3, amidine and triethylamine in benzene under reflux for 3 h; further addn. of triethylamine after 1.5 h; cooling; filtration;; evapn. to dryness under reduced pressure; crystn. from CH2Cl2/methanol; filtration; washing with methanol, water, methanol and light petroleum; drying in vac.; elem. anal.;
DOI:10.1039/DT9930002827

Reference yield:

: 24846-85-3,28060-70-0,77448-67-0,16971-01-0
IrHCl2(PPh3)3

: 6944-19-0
N,N'-diphenylpropionimidamide

: 143202-26-0
IrHCl(C₆H₅NC(C₂H₅)NC₆H₅)(P(C₆H₅)3)2

Guidance literature:: With triethylamine; In benzene; reaction of Ir-complex and N,N'-diphenylamidine in refluxing benzene in presence of NEt3;
DOI:10.1016/S0277-5387(00)83353-7