C₆₆H₉₅ClN₁₀O₁₄S

Base Information

Chemical Name:C₆₆H₉₅ClN₁₀O₁₄S
CAS No.:1374429-86-3
Molecular Formula:C₆₆H₉₅ClN₁₀O₁₄S
Molecular Weight:1320.06
Hs Code.:

C<sub>66</sub>H<sub>95</sub>ClN<sub>10</sub>O<sub>14</sub>S

Synonyms:

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Chemical Property of C₆₆H₉₅ClN₁₀O₁₄S

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Technology Process of C₆₆H₉₅ClN₁₀O₁₄S

There total 3 articles about C₆₆H₉₅ClN₁₀O₁₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374429-84-1
C₅₀H₆₈ClN₇O₉

: 1374429-86-3
C₆₆H₉₅ClN₁₀O₁₄S

Guidance literature:: Multi-step reaction with 2 steps

1: methoxybenzene; trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C

With methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2012.03.012

Reference yield:

: 1393687-43-8,133970-31-7
Fmoc-D-Lys(2-Cl-Z)-OH

: 1374429-86-3
C₆₆H₉₅ClN₁₀O₁₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-hydroxy-7-aza-benzotriazole; benzotriazol-1-ol; diisopropyl-carbodiimide / N,N-dimethyl-formamide / solid phase reaction

1.2: solid phase reaction

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane / 2.5 h / Inert atmosphere

3.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C

With 1-hydroxy-7-aza-benzotriazole; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.03.012

Reference yield:

: 1374429-82-9
NH₂-Phe-Me-D-Phe-D-Lys(2-Cl-Z)-Lys(Boc)-Leu-OH

: 1374429-86-3
C₆₆H₉₅ClN₁₀O₁₄S

Guidance literature:: Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane / 2.5 h / Inert atmosphere

2: methoxybenzene; trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In dichloromethane;
DOI:10.1016/j.bmcl.2012.03.012