ClCo(C₆H₈NOHNO)2((C₆H₅)3P)

Base Information

Chemical Name:ClCo(C₆H₈NOHNO)2((C₆H₅)3P)
CAS No.:245111-04-0
Molecular Formula:C₃₀H₃₃ClCoN₄O₄P
Molecular Weight:639.036
Hs Code.:

ClCo(C<sub>6</sub>H<sub>8</sub>NOHNO)2((C<sub>6</sub>H<sub>5</sub>)3P)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ClCo(C₆H₈NOHNO)2((C₆H₅)3P)

Chemical Property:

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Technology Process of ClCo(C₆H₈NOHNO)2((C₆H₅)3P)

There total 1 articles about ClCo(C₆H₈NOHNO)2((C₆H₅)3P) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cobalt(II) chloride hexahydrate

: 492-99-9
1,2-cyclohexanedionedioxime

: 603-35-0
triphenylphosphine

: 245111-04-0
ClCo(C₆H₈NOHNO)2((C₆H₅)3P)

Guidance literature:: With O₂ (air); In ethanol; byproducts: (C6H5)3P*HCl, H2O; addn. with constant stirring of triphenylphosphine to refluxing soln. of CoCl2*6H2O and C6H8(NOH)2 in ethanol; cooling to room temp.; passing air through react. mixt. for 6 h; pptn., filtration, washing with ethanol, ether; drying; purifn. by silica gel column using chloroform-ethylacetate; elem. anal.;
DOI:10.1016/S0022-328X(00)00380-6

Reference yield:

: sodium azide

: 245111-04-0
ClCo(C₆H₈NOHNO)2((C₆H₅)3P)

: 70106-19-3
N₃Co(C₆H₈NOHNO)2((C₆H₅)3P)

Guidance literature:: In methanol; water; byproducts: NaCl; addn. of aq. soln. of NaN3 to refluxing suspn. of ClCO(chgH)2PPh3 in methanol; reflux for 2 h; rotary evapn., filtration; washing with methanol, pet ether, drying, purifn. by silica gel column using chloroform-ethylacetate; elem. anal.;
DOI:10.1016/S0022-328X(00)00380-6