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Technology Process of (C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2

(C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2

Base Information
  • Chemical Name:(C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2
  • CAS No.:170242-43-0
  • Molecular Formula:C36H34Cl2Zr
  • Molecular Weight:628.796
  • Hs Code.:
(C<sub>5</sub>H<sub>5</sub>)(C<sub>13</sub>H<sub>7</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)2)ZrCl<sub>2</sub>

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Chemical Property of (C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2
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Technology Process of (C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2

There total 1 articles about (C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopentadienylzirconium trichloride

cyclopentadienylzirconium trichloride

2,7-dimesitylfluorene
170242-36-1

2,7-dimesitylfluorene

(C<sub>5</sub>H<sub>5</sub>)(C<sub>13</sub>H<sub>7</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)2)ZrCl<sub>2</sub>
170242-43-0

(C5H5)(C13H7(C6H2(CH3)3)2)ZrCl2

Guidance literature:
With BuLi; In diethyl ether; hexane; byproducts: LiCl, butane; Ar-atmosphere; treatment of ligand precursor (in Et2O) with BuLi (in hexane) at room temp., addn. of Zr-complex, stirring for 1 h; solvent removal, extn. into PhMe, filtration over Na2SO4, concn., crystn. (-78°C);
DOI:10.1016/0022-328X(95)05640-B
upstream raw materials:

2,7-dimesitylfluorene

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