brex-4-ene

Base Information

Chemical Name:brex-4-ene
CAS No.:15782-76-0
Molecular Formula:C₉H₁₂
Molecular Weight:120.194
Hs Code.:

Synonyms:

Suppliers and Price of brex-4-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of brex-4-ene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of brex-4-ene

There total 2 articles about brex-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 53439-36-4,77844-45-2,102130-72-3
endo-5-brexanol

: 6567-11-9
deltacyclane

: 15782-76-0
brex-4-ene

Guidance literature:: With potassium hydrogensulfate; at 130 - 150 ℃; under 105 Torr; Yields of byproduct given;

Reference yield:

: 14805-44-8,66808-05-7,87507-46-8,87507-47-9,87507-48-0,87507-49-1,148810-15-5
exo-brendan-2-ol

: 6567-11-9
deltacyclane

: 15782-76-0
brex-4-ene

Guidance literature:: With potassium hydrogensulfate; at 130 - 150 ℃; under 105 Torr; Yields of byproduct given;

Reference yield:

: 15782-76-0
brex-4-ene

: 77787-42-9,77844-46-3
endo-brexan-5-ol p-bromobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) mercuric acetate; 2.) pyridine / 1.) water, tetrahydrofuran; 2.) 8 h, r.t., water, tetrahydrofuran

2: 90 percent / lithium aluminium hydride / diethyl ether / 13 h / Ambient temperature

3: 99 percent / 1.) methyl lithium / diethyl ether / 1.) 10 min,; 2.) 1 h

With pyridine; lithium aluminium tetrahydride; mercury(II) diacetate; methyllithium; In diethyl ether;