C₃₀H₂₇NO₇S

Base Information

• Chemical Name: C₃₀H₂₇NO₇S
• CAS No.: 138785-13-4
• Molecular Formula: C₃₀H₂₇NO₇S
• Molecular Weight: 545.613
• Mol file: 138785-13-4.mol

Synonyms:

Chemical Property of C₃₀H₂₇NO₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₇NO₇S

There total 8 articles about C₃₀H₂₇NO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C30H27NO5S (144127-42-4) → C30H27NO7S (138785-13-4,141395-24-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 0.5h;

DOI:10.1021/ja00049a022

Reference yield:

C26H19NO4 (130031-63-9) → C30H27NO7S (138785-13-4,141395-24-6)

Guidance literature:

Multi-step reaction with 8 steps

1: 92 percent / cesium carbonate, 18-crown-6 / acetonitrile / 10 h / Ambient temperature

2: 0.5 N aq. LiOH / tetrahydrofuran / 0.5 h / 0 °C

3: triphenylphosphine / CH₂Cl₂ / 0.5 h / 0 °C

4: 68 percent / sodium borohydride / CH₂Cl₂; propan-2-ol / 0.5 h / 0 °C

5: 99 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / -78 - 0 °C

6: 98 percent / NaH / tetrahydrofuran / 0.08 h / 0 °C

7: 96 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

8: 82 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

With 2,6-dimethylpyridine; lithium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; tetrabutyl ammonium fluoride; sodium hydride; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; isopropyl alcohol; acetonitrile;

DOI:10.1021/ja00049a022

Reference yield:

C28H23NO5 (132938-56-8) → C30H27NO7S (138785-13-4,141395-24-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 99 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / -78 - 0 °C

2: 98 percent / NaH / tetrahydrofuran / 0.08 h / 0 °C

3: 96 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

4: 82 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00049a022

upstream raw materials:

C₃₀H₂₇NO₅S

C₂₆H₁₉NO₄

C₂₈H₂₃NO₅

C₃₃H₂₄N₂O₅S

Downstream raw materials:

C₁₀₆H₁₄₈IN₃O₂₅S₂Si₄

C₁₀₆H₁₄₈IN₃O₂₅S₂Si₄

C₁₀₆H₁₄₈IN₃O₂₅S₂Si₄

C₁₀₆H₁₄₈IN₃O₂₅S₂Si₄