(3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole

Base Information

• Chemical Name: (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole
• CAS No.: 1420481-73-7
• Molecular Formula: C₂₇H₃₆O₄Se
• Molecular Weight: 503.54

Synonyms:

Chemical Property of (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole

Chemical Property:

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Technology Process of (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole

There total 4 articles about (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H42O10S2 (1420479-87-3) → (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole (1420481-73-7)

Guidance literature:

With selenium; sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 0 ℃; for 72h; Inert atmosphere; Reflux;

DOI:10.1021/ja311202e

Reference yield:

1,2;5,6-dianhydro-3,4-O-isopropylidene-D-mannitol (63700-05-0) → (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole (1420481-73-7)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12.1 h / 0 - 25 °C / Inert atmosphere

3: selenium; sodium tetrahydroborate / ethanol; tetrahydrofuran / 72 h / 0 °C / Inert atmosphere; Reflux

With selenium; sodium tetrahydroborate; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja311202e

Reference yield:

4-Isopropylphenol (99-89-8) → (3aS,4S,6S,6aS)-4,6-bis((4-isopropylphenoxy)methyl)-2,2-dimethyltetrahydroselenopheno[3,4-d][1,3]dioxole (1420481-73-7)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12.1 h / 0 - 25 °C / Inert atmosphere

3: selenium; sodium tetrahydroborate / ethanol; tetrahydrofuran / 72 h / 0 °C / Inert atmosphere; Reflux

With selenium; sodium tetrahydroborate; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja311202e

upstream raw materials:

1,2;5,6-dianhydro-3,4-O-isopropylidene-D-mannitol

4-Isopropylphenol

C₂₉H₄₂O₁₀S₂

C₂₇H₃₈O₆

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