C₃₅H₄₄N₄O₄S

Base Information

Chemical Name:C₃₅H₄₄N₄O₄S
CAS No.:1609109-68-3
Molecular Formula:C₃₅H₄₄N₄O₄S
Molecular Weight:616.825
Hs Code.:

C<sub>35</sub>H<sub>44</sub>N<sub>4</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₃₅H₄₄N₄O₄S

Chemical Property:

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Technology Process of C₃₅H₄₄N₄O₄S

There total 8 articles about C₃₅H₄₄N₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-10-2
benzenesulfonamide

: 1609109-77-4
C₂₉H₃₉N₃O₃

: 1609109-68-3
C₃₅H₄₄N₄O₄S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.bmcl.2014.03.090

Reference yield:

: 1609109-71-8
C₁₂H₁₄O₃

: 1609109-68-3
C₃₅H₄₄N₄O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: zinc; iodine / 20 °C / Sonication

2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

3: potassium trimethylsilonate / tetrahydrofuran / 20 °C

4: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

5: camphor-10-sulfonic acid / ethyl acetate / 80 °C

6: lithium hydroxide; water / tetrahydrofuran; methanol / 20 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With triethylsilane; dmap; boron trifluoride diethyl etherate; potassium trimethylsilonate; water; iodine; camphor-10-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; lithium hydroxide; zinc; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1: |Reformatsky Reaction;
DOI:10.1016/j.bmcl.2014.03.090

Reference yield:

: 1609109-74-1
C₁₈H₂₆O₄

: 1609109-68-3
C₃₅H₄₄N₄O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: potassium trimethylsilonate / tetrahydrofuran / 20 °C

2: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

3: camphor-10-sulfonic acid / ethyl acetate / 80 °C

4: lithium hydroxide; water / tetrahydrofuran; methanol / 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With dmap; potassium trimethylsilonate; water; camphor-10-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.03.090