Technology Process of C23H20ClN3O
There total 15 articles about C23H20ClN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1016/j.bmcl.2013.12.068
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 80 ℃;
DOI:10.1016/j.bmcl.2013.12.068
- Guidance literature:
-
Multi-step reaction with 7 steps
1: bis(tri-t-butylphosphine)palladium(0); potassium fluoride / tetrahydrofuran / 100 °C
2: tin(ll) chloride / ethanol / 75 °C
3: acetic acid
4: silver nitrate / 75 °C
5: potassium carbonate / N,N-dimethyl-formamide
6: sodium hydroxide / water
7: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
With
potassium fluoride; bis(tri-t-butylphosphine)palladium(0); benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; silver nitrate; acetic acid; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.068
