phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside

Base Information

• Chemical Name: phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside
• CAS No.: 1021159-92-1
• Molecular Formula: C₃₆H₄₈N₂O₁₉
• Molecular Weight: 812.779

Synonyms:

Chemical Property of phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Useful:

Technology Process of phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside

There total 1 articles about phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (2S,3R,4S,5R,6R)-4-acetoxy-5-hydroxy-6-hydroxymethyl-2-phenoxy-tetrahydro-pyran-3-yl ester (23740-56-9) + (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosonamide) 2-O-(diethyl phosphite) (1021159-60-3) → phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside + phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside (1021159-92-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -40 ℃;

DOI:10.1021/jo702609p

Reference yield:

phenyl (N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonamide)-(2->6)-2,3-di-O-acetyl-β-D-glucopyranoside (1021159-92-1) → C24H36N2O13

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 1h;

DOI:10.1021/jo702609p

upstream raw materials:

Acetic acid (2S,3R,4S,5R,6R)-4-acetoxy-5-hydroxy-6-hydroxymethyl-2-phenoxy-tetrahydro-pyran-3-yl ester

(N-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosonamide) 2-O-(diethyl phosphite)

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