benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

• Chemical Name: benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside
• CAS No.: 142644-75-5
• Molecular Formula: C₁₀₄H₁₁₀O₂₀
• Molecular Weight: 1680.01
• Mol file: 142644-75-5.mol

Synonyms:

Chemical Property of benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside

There total 1 articles about benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-deoxy-1-(S-ethyl)-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside (74666-83-4,105990-37-2,125354-46-3,125354-47-4,125411-99-6,108739-67-9) + bnezyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside (142644-74-4) → benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside (142644-79-9) + benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside (142644-75-5)

Guidance literature:

With molecular sieve; methyl trifluoromethanesulfonate; In diethyl ether; for 16h;

DOI:10.1016/S0008-6215(00)90488-9

Reference yield: 51.0%

benzyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside (142644-75-5) → benzyl 3-O-<4-O-(3-O-allyl-6-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside (142644-76-6)

Guidance literature:

With hydrogenchloride; molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; for 1h;

DOI:10.1016/S0008-6215(00)90488-9

upstream raw materials:

1-deoxy-1-(S-ethyl)-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

bnezyl 3-O-<4-O-(3-O-allyl-4,6-O-benzylidene-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside

Downstream raw materials:

benzyl 3-O-<4-O-(3-O-allyl-6-O-benzyl-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranosyl>-2,4-di-O-benzyl-α-L-rhamnopyranoside