C₃₉H₄₉NO₁₄S

Base Information

Chemical Name:C₃₉H₄₉NO₁₄S
CAS No.:1373514-05-6
Molecular Formula:C₃₉H₄₉NO₁₄S
Molecular Weight:787.882
Hs Code.:

C<sub>39</sub>H<sub>49</sub>NO<sub>14</sub>S

Synonyms:

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Chemical Property of C₃₉H₄₉NO₁₄S

Chemical Property:

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Technology Process of C₃₉H₄₉NO₁₄S

There total 11 articles about C₃₉H₄₉NO₁₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130266-57-8
2-methoxyacridine-9-carboxylic acid

: 1373514-05-6
C₃₉H₄₉NO₁₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere

2.1: boron tribromide / dichloromethane / 4 h / 20 °C

2.2: 16 h / 0 - 20 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4.1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid

5.1: hydrogenchloride / water / 1.5 h / Reflux; Inert atmosphere

With pyridine; hydrogenchloride; 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; boron tribromide; p-toluenesulfonyl chloride; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 3.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1373514-05-6
C₃₉H₄₉NO₁₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 145 °C / Inert atmosphere

2.1: potassium hydroxide / water / 4 h / Inert atmosphere; Reflux

3.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 4 h / 20 °C

4.2: 16 h / 0 - 20 °C

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

6.1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid

7.1: hydrogenchloride / water / 1.5 h / Reflux; Inert atmosphere

With pyridine; hydrogenchloride; 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; boron tribromide; sodium hydride; p-toluenesulfonyl chloride; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 5.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a

Reference yield:

: 42293-38-9
C₉H₉ClO₂

: 1373514-05-6
C₃₉H₄₉NO₁₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 48 h / 20 °C / Inert atmosphere

2.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 4 h / 20 °C

3.2: 16 h / 0 - 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5.1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid

6.1: hydrogenchloride / water / 1.5 h / Reflux; Inert atmosphere

With pyridine; hydrogenchloride; 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; boron tribromide; p-toluenesulfonyl chloride; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 4.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a