(3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate

Base Information

Chemical Name:(3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate
CAS No.:19775-56-5
Molecular Formula:C₂₄H₃₀N₂O₄
Molecular Weight:410.513
Hs Code.:

Synonyms:

Suppliers and Price of (3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate

Chemical Property:

Vapor Pressure:9.21E-11mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate

There total 15 articles about (3xi,16xi,21alpha)-ajmalan-17,21-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.6%

: 210533-31-6
2-epihydroxydiacetylajmaline

: 19775-56-5
diacetyl ajmaline

: 2-epidiacetylajmaline

Guidance literature:: With boron trifluoride diethyl etherate; hydrogen; platinum(IV) oxide; In dichloromethane; for 24h; under 760 Torr;
DOI:10.1021/ja990184l

Reference yield:

: 143065-03-6
(6S,8S,9S,10S,1'S)-5-methyl-8-(1'-ethyl-oxomethyl)-9-(1',3'-dioxolan-2'-yl)-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooct[b]-indole

: 19775-56-5
diacetyl ajmaline

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10 percent Pd/C / 1,2-dimethoxy-ethane / 48 h / 760 Torr

2: DMAP / 1,2-dimethoxy-ethane / 2 h

3: aq. conc. HCl / acetic acid / 3 h / Ambient temperature

4: HCl(g) / 48 h / Ambient temperature

5: 35.6 percent / BF₃*Et₂O, H₂ / PtO₂ / CH₂Cl₂ / 24 h / 760 Torr

With hydrogenchloride; dmap; boron trifluoride diethyl etherate; hydrogen; platinum(IV) oxide; palladium on activated charcoal; In 1,2-dimethoxyethane; dichloromethane; acetic acid;
DOI:10.1021/ja990184l

Reference yield:

: 210533-30-5
21-O-acetylajmalal A ethylene acetal

: 19775-56-5
diacetyl ajmaline

Guidance literature:: Multi-step reaction with 3 steps

1: aq. conc. HCl / acetic acid / 3 h / Ambient temperature

2: HCl(g) / 48 h / Ambient temperature

3: 35.6 percent / BF₃*Et₂O, H₂ / PtO₂ / CH₂Cl₂ / 24 h / 760 Torr

With hydrogenchloride; boron trifluoride diethyl etherate; hydrogen; platinum(IV) oxide; In dichloromethane; acetic acid;
DOI:10.1021/ja990184l