1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Base Information

Chemical Name:1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid
CAS No.:1394857-16-9
Molecular Formula:C₂₇H₂₄O₉
Molecular Weight:492.482
Hs Code.:

Synonyms:

Suppliers and Price of 1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

There total 3 articles about 1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1394857-15-8
1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronamide

: 1394857-16-9
1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Guidance literature:: With acetic acid; isopentyl nitrite; at 90 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jo300722y

Reference yield:

: 915154-60-8
3-O-benzyl-1,2-O-isopropylidene-α-L-idofuranonitrile

: 1394857-16-9
1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / tetrahydrofuran / 4 h / 0 - 20 °C

2: dmap / dichloromethane; tetrahydrofuran / 8 h

3: isopentyl nitrite; acetic acid / 5 h / 90 °C / Inert atmosphere

With hydrogenchloride; dmap; water; acetic acid; isopentyl nitrite; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo300722y

Reference yield:

: 3-O-benzyl-L-idopyranuronamide

: 1394857-16-9
1,2-di-O-benzoyl-3-O-benzyl-β-L-idopyranuronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane; tetrahydrofuran / 8 h

2: isopentyl nitrite; acetic acid / 5 h / 90 °C / Inert atmosphere

With dmap; acetic acid; isopentyl nitrite; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo300722y