Technology Process of C32H37ClN2O2S
There total 9 articles about C32H37ClN2O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / Reflux
2: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C
3: ethanol / Reflux
4: boron tribromide / dichloromethane / -78 °C
5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
With
sodium hydrogen sulfide; di-isopropyl azodicarboxylate; boron tribromide; potassium carbonate; triphenylphosphine; magnesium chloride;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
5: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.10.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C
2: ethanol / Reflux
3: boron tribromide / dichloromethane / -78 °C
4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
With
sodium hydrogen sulfide; di-isopropyl azodicarboxylate; boron tribromide; triphenylphosphine; magnesium chloride;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
4: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.10.022
