C₂₅H₂₇ClN₂O₂

Base Information

Chemical Name:C₂₅H₂₇ClN₂O₂
CAS No.:116171-94-9
Molecular Formula:C₂₅H₂₇ClN₂O₂
Molecular Weight:422.955
Hs Code.:

C<sub>25</sub>H<sub>27</sub>ClN<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₇ClN₂O₂

Chemical Property:

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Technology Process of C₂₅H₂₇ClN₂O₂

There total 9 articles about C₂₅H₂₇ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107688-26-6,116260-70-9,116260-74-3
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaurenitril

: 116171-94-9
C₂₅H₂₇ClN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / sodium hydroxide, 30percent hydrogen peroxide / ethanol / 3 h / Ambient temperature

2: 77 percent / Amberlyst 15 / 120 h / 60 °C

3: sodium hydroxide, water, ethyl acetate, HCl / ethanol / 100 h / 100 °C

4: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

5: 69 percent / H₂, / 10percent Pd/C / ethyl acetate / 1 h / 40 - 50 °C

6: triethylamine, butylhypochlorit sol. / CH₂Cl₂; CCl₄

With hydrogenchloride; sodium hydroxide; Amberlyst 15; normal butyl hypochlorite; water; hydrogen; dihydrogen peroxide; ethyl acetate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrachloromethane; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 116171-86-9
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeure

: 116171-94-9
C₂₅H₂₇ClN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

2: 69 percent / H₂, / 10percent Pd/C / ethyl acetate / 1 h / 40 - 50 °C

3: triethylamine, butylhypochlorit sol. / CH₂Cl₂; CCl₄

With normal butyl hypochlorite; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrachloromethane; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 107688-27-7,116260-78-7,116262-35-2
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-7-carbonsaureamid

: 116171-94-9
C₂₅H₂₇ClN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / Amberlyst 15 / 120 h / 60 °C

2: sodium hydroxide, water, ethyl acetate, HCl / ethanol / 100 h / 100 °C

3: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

4: 69 percent / H₂, / 10percent Pd/C / ethyl acetate / 1 h / 40 - 50 °C

5: triethylamine, butylhypochlorit sol. / CH₂Cl₂; CCl₄

With hydrogenchloride; sodium hydroxide; Amberlyst 15; normal butyl hypochlorite; water; hydrogen; ethyl acetate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrachloromethane; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86863-0