sortin1

Base Information

• Chemical Name: sortin1
• CAS No.: 503837-98-7
• Molecular Formula: C₂₆H₁₉NO₆
• Molecular Weight: 441.44
• Mol file: 503837-98-7.mol

Synonyms:

Chemical Property of sortin1

Chemical Property:

• Boiling Point: 675.4±55.0 °C(Predicted)
• PKA: 4.18±0.10(Predicted)
• Density: 1.45±0.1 g/cm3(Predicted)

Purity/Quality:

≥95% ^*data from raw suppliers

Sortin1 98+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sortin1

There total 4 articles about sortin1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C27H21NO6 → sortin1 (503837-98-7)

Guidance literature:

With lithium hydroxide monohydrate; water; In methanol; at 40 ℃; for 1h;

DOI:10.1016/j.bmcl.2018.03.060

Reference yield:

5-bromo-2-furancarboxaldehyde (1899-24-7) → sortin1 (503837-98-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate; palladium diacetate / water; acetone / 0.42 h / 20 °C

2.1: acetic acid / 0.08 h / 110 °C

2.2: 0.02 h / 110 °C

3.1: lithium hydroxide monohydrate; water / methanol / 1 h / 40 °C

With lithium hydroxide monohydrate; water; palladium diacetate; sodium carbonate; acetic acid; In methanol; water; acetone; 1.1: |Suzuki-Miyaura Coupling;

DOI:10.1016/j.bmcl.2018.03.060

Reference yield:

4-methoxycarbonylphenylboronic acid (99768-12-4) → sortin1 (503837-98-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate; palladium diacetate / water; acetone / 0.42 h / 20 °C

2.1: acetic acid / 0.08 h / 110 °C

2.2: 0.02 h / 110 °C

3.1: lithium hydroxide monohydrate; water / methanol / 1 h / 40 °C

With lithium hydroxide monohydrate; water; palladium diacetate; sodium carbonate; acetic acid; In methanol; water; acetone; 1.1: |Suzuki-Miyaura Coupling;

DOI:10.1016/j.bmcl.2018.03.060

upstream raw materials:

5-bromo-2-furancarboxaldehyde

4-methoxycarbonylphenylboronic acid

4-(5-formyl-2-furanyl)benzoic acid methyl ester

Refernces