4-methoxycarbonyl-1-pyridinium ylide

Base Information

Chemical Name:4-methoxycarbonyl-1-pyridinium ylide
CAS No.:160857-53-4
Molecular Formula:C₁₅H₁₅N₃O₅S
Molecular Weight:349.367
Hs Code.:

4-methoxycarbonyl-1-<p-(acetylamino)benzenesulphonylimino>pyridinium ylide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxycarbonyl-1-pyridinium ylide

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Technology Process of 4-methoxycarbonyl-1-pyridinium ylide

There total 1 articles about 4-methoxycarbonyl-1-pyridinium ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 4-methoxycarbonyl-N-aminopyridinium perchlorate

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 160857-53-4
4-methoxycarbonyl-1-pyridinium ylide

Guidance literature:: With sodium hydroxide; for 96h; Ambient temperature;

Reference yield: 67.0%

: 160857-53-4
4-methoxycarbonyl-1-pyridinium ylide

: 160857-54-5
p-acetylamino-N-<4-methoxycarbonyl-1.2.5.6-tetrahydro-1-pyridyl>benzenesulphonamide

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 12h;

Reference yield:

: 160857-53-4
4-methoxycarbonyl-1-pyridinium ylide

: N-(4-{4-[5-(4-Chloro-phenyl)-[1,3,4]oxadiazol-2-yl]-3,6-dihydro-2H-pyridin-1-ylsulfamoyl}-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / sodium borohydride / ethanol / 12 h

2: 34 percent / hydrazine hydrate (99percent) / 5 h

3: glacid acetic acid / methanol / Heating

4: lead dioxide / acetic acid / 6 h / Ambient temperature

With sodium tetrahydroborate; hydrazine hydrate; lead dioxide; acetic acid; In methanol; ethanol; acetic acid;