C₁₈H₁₇ClN₂O₂

Base Information

Chemical Name:C₁₈H₁₇ClN₂O₂
CAS No.:1426937-57-6
Molecular Formula:C₁₈H₁₇ClN₂O₂
Molecular Weight:328.798
Hs Code.:

C<sub>18</sub>H<sub>17</sub>ClN<sub>2</sub>O<sub>2</sub>

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Chemical Property of C₁₈H₁₇ClN₂O₂

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Technology Process of C₁₈H₁₇ClN₂O₂

There total 5 articles about C₁₈H₁₇ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.2%

: 1426937-32-7
N′-acetyl-2-(3-(4-chloro-3,5-dimethylphenoxy)phenyl)acetohydrazide

: 1426937-57-6
C₁₈H₁₇ClN₂O₂

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide; at 110 ℃; for 1h;
DOI:10.1021/jm400012e

Reference yield:

: 88-04-0
4-Chloro-3,5-dimethylphenol

: 1426937-57-6
C₁₈H₁₇ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; caesium carbonate; dimethylaminoacetic acid / 1,4-dioxane / 9 h / 180 °C

2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 5 h / 20 °C

4: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 110 °C

With copper(l) iodide; dimethylaminoacetic acid; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; 1: |Ullmann Condensation;
DOI:10.1021/jm400012e

Reference yield:

: 150529-73-0
methyl 2-(3-bromophenyl)acetatee

: 1426937-57-6
C₁₈H₁₇ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; caesium carbonate; dimethylaminoacetic acid / 1,4-dioxane / 9 h / 180 °C

2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 5 h / 20 °C

4: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 110 °C

With copper(l) iodide; dimethylaminoacetic acid; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; 1: |Ullmann Condensation;
DOI:10.1021/jm400012e