(C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)

Base Information

• Chemical Name: (C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)
• CAS No.: 391879-38-2
• Molecular Formula: C₆H₁₆N*C₁₇H₁₇Cl₇MoN₃
• Molecular Weight: 709.653

Synonyms:

Chemical Property of (C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)

There total 1 articles about (C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tetrachlorobis(tetrahydrofurano)molybdenum(IV) (16998-75-7) + (Cl2C6H3NHCH2CH2)2NCH3 (391879-59-7) + triethylamine (121-44-8) → (C2H5)3NH(1+)*(((Cl2C6H3NCH2CH2)2NCH3)MoCl3)(1-)=((C2H5)3NH)(((Cl2C6H3NCH2CH2)2NCH3)MoCl3) (391879-38-2)

Guidance literature:

In tetrahydrofuran; byproducts: Et3NHCl; MoCl4(THF)2 was added to stirring soln. ligand in THF and stirred for 10min, NEt3 was added dropwise and stirred for 3 h; ppt. was filtered off, filtrate was evapd. to dryness, washed with Et2O and crystd. from THF-Et2O 1:1 at -30°C; elem. anal.;

DOI:10.1021/om0106985

Reference yield: 87.0%

(C2H5)3NH(1+)*(((Cl2C6H3NCH2CH2)2NCH3)MoCl3)(1-)=((C2H5)3NH)(((Cl2C6H3NCH2CH2)2NCH3)MoCl3) (391879-38-2) + tetrabutyl-ammonium chloride (1112-67-0) → (C4H9)4N(1+)*(((Cl2C6H3NCH2CH2)2NCH3)MoCl3)(1-)=((C4H9)4N)(((Cl2C6H3NCH2CH2)2NCH3)MoCl3) (391879-70-2)

Guidance literature:

In tetrahydrofuran; byproducts: Et3NHCl; Bu4NCl was added to stirring soln. Mo complex in THF and stired overnight; THF was removed in vacuo, residue was extd. with benzene and filtered, solvent was removed; elem. anal.;

DOI:10.1021/om0106985

Reference yield: 79.0%

(C2H5)3NH(1+)*(((Cl2C6H3NCH2CH2)2NCH3)MoCl3)(1-)=((C2H5)3NH)(((Cl2C6H3NCH2CH2)2NCH3)MoCl3) (391879-38-2) + (trimethylsilyl)methylmagnesium chloride (13170-43-9) → (((Cl2C6H3NCH2CH2)2NCH3)Mo(CH2Si(CH3)3)2) (391879-42-8)

Guidance literature:

In tetrahydrofuran; Me3SiCH2MgCl was added dropwise to stirring soln. Mo complex in THF at -30°C and stirred at room temp. for 90 min; volatiles were removed in vacuo, Et2O was added to residue followed by 1,4-dioxane, stirred for 10 min and filtered, filtrate was concd. and filtered, pentane was added and stored at -30°C overnight; elem. anal.;

DOI:10.1021/om0106985

upstream raw materials:

tetrachlorobis(tetrahydrofurano)molybdenum(IV)

(Cl₂C₆H₃NHCH₂CH₂)2NCH₃

triethylamine

Downstream raw materials:

(C₄H₉)4N⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₄H₉)4N)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)

(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)Mo(CH₂Si(CH₃)3)2)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 391879-38-2 (C₂H₅)3NH⁽¹⁺⁾*(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)^(1-)=((C₂H₅)3NH)(((Cl₂C₆H₃NCH₂CH₂)2NCH₃)MoCl₃)

Send

Send

Metric Ton KG G Pound L ML

Send

Send