all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

Base Information

Chemical Name:all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane
CAS No.:180306-22-3
Molecular Formula:C₃₂H₅₆O₈
Molecular Weight:568.792
Hs Code.:

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Chemical Property of all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

Chemical Property:

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Technology Process of all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

There total 8 articles about all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₇₂O₁₀

: 180306-22-3
all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 60 ℃; for 4h;

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 180306-22-3
all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / sodium methoxide, sodium iodide / ethanol / 16 h / Heating

2: 60 percent / sodium hydroxide, potassium hydroxide / ethanol; H₂O / 1 h / 200 °C

3: pyridinium 4-toluenesulfonate / CH₂Cl₂ / 24 h / Ambient temperature

4: 30 g / potassium hydroxide / H₂O / 3 h / Heating

5: triethylamine / CH₂Cl₂ / 3 h

6: 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -30 deg C, 1 h, 2.) room temperature, overnight

7: 2.5 g / pyridinium 4-toluenesulfonate / ethanol / 4 h / 60 °C

With dmap; potassium hydroxide; sodium hydroxide; sodium methylate; pyridinium p-toluenesulfonate; triethylamine; sodium iodide; In ethanol; dichloromethane; water;

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 180306-22-3
all-trans-1,4-bis-[4-(6-hydroxyhexyloxy)cyclohexanecarbonyloxy]cyclohexane

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / sodium methoxide, sodium iodide / ethanol / 16 h / Heating

2: 60 percent / sodium hydroxide, potassium hydroxide / ethanol; H₂O / 1 h / 200 °C

3: pyridinium 4-toluenesulfonate / CH₂Cl₂ / 24 h / Ambient temperature

4: 30 g / potassium hydroxide / H₂O / 3 h / Heating

5: triethylamine / CH₂Cl₂ / 3 h

6: 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -30 deg C, 1 h, 2.) room temperature, overnight

7: 2.5 g / pyridinium 4-toluenesulfonate / ethanol / 4 h / 60 °C

With dmap; potassium hydroxide; sodium hydroxide; sodium methylate; pyridinium p-toluenesulfonate; triethylamine; sodium iodide; In ethanol; dichloromethane; water;