5,10-Dimethylbenzo[g]isoquinoline

Base Information

• Chemical Name: 5,10-Dimethylbenzo[g]isoquinoline
• CAS No.: 33301-42-7
• Molecular Formula: C₁₅H₁₃N
• Molecular Weight: 207.275
• NSC Number: 151467
• DSSTox Substance ID: DTXSID60302496
• Nikkaji Number: J1.024.577J
• Wikidata: Q82047295
• Mol file: 33301-42-7.mol

Synonyms:5,10-dimethylbenzo[g]isoquinoline;33301-42-7;NSC151467;SCHEMBL1102485;DTXSID60302496;NSC 151467;NSC-151467;A821795

Chemical Property of 5,10-Dimethylbenzo[g]isoquinoline

Chemical Property:

• Vapor Pressure: 8.52E-06mmHg at 25°C
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 207.104799419
• Heavy Atom Count: 16
• Complexity: 250

Purity/Quality:

99% ，98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C2C=CN=CC2=C(C3=CC=CC=C13)C

Technology Process of 5,10-Dimethylbenzo[g]isoquinoline

There total 2 articles about 5,10-Dimethylbenzo[g]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

5,10-Dimethyl-5,10-dihydro-benzo[g]isoquinoline-5,10-diol → 9,10-dimethylbenz[g]isoquinoline (33301-42-7)

Guidance literature:

With hydrogen iodide; acetic acid; at 140 ℃; for 5h;

DOI:10.1002/jhet.5570350328

Reference yield: 44.0%

1-[4-(1-Phenyl-ethyl)-pyridin-3-yl]-ethanone (213212-52-3) → 9,10-dimethylbenz[g]isoquinoline (33301-42-7)

Guidance literature:

With PPA; at 140 ℃; for 1.5h;

DOI:10.1002/jhet.5570350328

upstream raw materials:

1-[4-(1-Phenyl-ethyl)-pyridin-3-yl]-ethanone