C₃₃H₄₄N₄O₉S

Base Information

Chemical Name:C₃₃H₄₄N₄O₉S
CAS No.:1414915-92-6
Molecular Formula:C₃₃H₄₄N₄O₉S
Molecular Weight:672.8
Hs Code.:

C<sub>33</sub>H<sub>44</sub>N<sub>4</sub>O<sub>9</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₄N₄O₉S

Chemical Property:

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Technology Process of C₃₃H₄₄N₄O₉S

There total 3 articles about C₃₃H₄₄N₄O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 1414915-90-4
C₂₈H₃₄N₆O₇S

: 1414915-92-6
C₃₃H₄₄N₄O₉S

Guidance literature:: With trimethylphosphane; In tetrahydrofuran; at -20 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm301058f

Reference yield:

: 132286-77-2
(S)-4-(allyloxy)-2-((tert-butoxycarbonyl)amino)-4-oxobutanoic acid

: 1414915-92-6
C₃₃H₄₄N₄O₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

3.1: hydrogen azide; triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane; toluene / -25 - -20 °C / Inert atmosphere

4.1: trimethylphosphane / tetrahydrofuran / 5 h / -20 - 20 °C / Inert atmosphere

With hydrogen azide; di-isopropyl azodicarboxylate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; trifluoroacetic acid; trimethylphosphane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm301058f

Reference yield:

: 99792-99-1
aspartic acid β-allyl ester

: 1414915-92-6
C₃₃H₄₄N₄O₉S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,4-dioxane; water

2.1: N-ethyl-N,N-diisopropylamine; HATU; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4.1: hydrogen azide; triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane; toluene / -25 - -20 °C / Inert atmosphere

5.1: trimethylphosphane / tetrahydrofuran / 5 h / -20 - 20 °C / Inert atmosphere

With hydrogen azide; di-isopropyl azodicarboxylate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; trifluoroacetic acid; trimethylphosphane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm301058f