C₂₃H₂₇NO₂

Base Information

Chemical Name:C₂₃H₂₇NO₂
CAS No.:1443436-92-7
Molecular Formula:C₂₃H₂₇NO₂
Molecular Weight:349.473
Hs Code.:

C<sub>23</sub>H<sub>27</sub>NO<sub>2</sub>

Synonyms:

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Chemical Property of C₂₃H₂₇NO₂

Chemical Property:

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Technology Process of C₂₃H₂₇NO₂

There total 6 articles about C₂₃H₂₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1085372-36-6
(E)-ethyl 3-(1-benzyl-4-ethyl-1H-indol-7-yl)but-2-enoate

: 1443436-92-7
C₂₃H₂₇NO₂

: C₂₃H₂₇NO₂

Guidance literature:: With C₄₅H₄₆IrNO₂P⁽¹⁺⁾*C₂₄H₁₂BF₈^(1-); In dichloromethane; at 40 ℃; for 14h; under 37503.8 Torr; Pressure; Temperature; Time; Solvent;
DOI:10.1002/chem.201202413

Reference yield:

: 161988-90-5
7-bromo-4-ethyl-1H-indole

: 1443436-92-7
C₂₃H₂₇NO₂

: C₂₃H₂₇NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h

1.2: 12 h / 20 °C

2.1: palladium dichloride; triethylamine; tris-(o-tolyl)phosphine / acetonitrile

3.1: C₄₅H₄₆IrNO₂P⁽¹⁺⁾*C₂₄H₁₂BF₈^(1-) / dichloromethane / 14 h / 40 °C / 37503.8 Torr

With C₄₅H₄₆IrNO₂P⁽¹⁺⁾*C₂₄H₁₂BF₈^(1-); triethylamine; tris-(o-tolyl)phosphine; potassium hydroxide; palladium dichloride; In dichloromethane; dimethyl sulfoxide; acetonitrile; 2.1: |Heck Reaction;
DOI:10.1002/chem.201202413

Reference yield:

: 18640-58-9
3-nitro-4-bromoacetophenone

: 1443436-92-7
C₂₃H₂₇NO₂

: C₂₃H₂₇NO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C

2.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 3 h / 0 °C

2.2: 0.5 h / 0 - 20 °C

3.1: tetrahydrofuran / 0.75 h / -45 °C / Schlenk technique; Inert atmosphere

4.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h

4.2: 12 h / 20 °C

5.1: palladium dichloride; triethylamine; tris-(o-tolyl)phosphine / acetonitrile

6.1: C₄₅H₄₆IrNO₂P⁽¹⁺⁾*C₂₄H₁₂BF₈^(1-) / dichloromethane / 14 h / 40 °C / 37503.8 Torr

With 1H-imidazole; sodium tetrahydroborate; C₄₅H₄₆IrNO₂P⁽¹⁺⁾*C₂₄H₁₂BF₈^(1-); iodine; triethylamine; triphenylphosphine; tris-(o-tolyl)phosphine; potassium hydroxide; palladium dichloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; 3.1: |Bartoli Indole Synthesis / 5.1: |Heck Reaction;
DOI:10.1002/chem.201202413